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Two-dimensional 1H-15N HMBC NMR spectra of a well-knownanticonvulsant-carbamazepine-dissolved in chloroform, recorded on an NMRspectrometer and obtained from quantum-chemical calculations prove theexistence of hidden conformers in saturated solutions. A weaker influence ofring currents was revealed for the hidden conformation of carbamazepinedissolved in saturated solution, which provides a simple approach fordiscovering hidden conformations. Hidden conformers were found in threedifferent solvents: dimethyl sulfoxide, chloroform, and dichloromethane.

Exposing Hidden Alternative Conformations of Small Flexible Molecules in 2D NMR Spectroscopy Using 1H-15N HMBC