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The magnetic properties of a novel cobalt-based hydrogen vanadate,Co13.5(OH)6(H0.5VO3.5)2(VO4)6, are reported. This new magnetic material wassynthesized in single-crystal form using a conventional hydrothermal method.Its crystal structure was determined from single-crystal X-ray diffraction dataand was also characterized by scanning electron microscopy. Its crystalframework has a dumortierite-like structure consisting of large hexagonal andtrigonal channels; the large hexagonal channels contain one-dimensional chainsof face-sharing CoO6 octahedra linked to the framework by rings of VO4tetrahedra, while the trigonal channels are occupied by chains of disorderedV2O4 pyramidal groups. The magnetic properties of this material wereinvestigated by DC magnetic measurements, which indicate the occurrence ofantiferromagnetic interactions.

Magnetic properties of a new cobalt hydrogen vanadate with a dumortierite-like structure: Co13.5(OH)6(H0.5VO3.5)2(VO4)6