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The three-dimensional structures of the primary Al3Sc particles in an Al-2Scmaster alloy were studied by synchrotron X-ray microtomography, scanning andtransmission electron microscopy. The Al3Sc phases were found to be a singlecube and a cluster of cubes. The surface area, equivalent diameter of the Al3Sccubes increased with the increasing of cube volume, but the specific surfacearea decreases. The primary Al3Sc cubes and Al-matrix have the same crystalorientation, indicating that the Al3Sc phases are the heterogeneous nucleationsites for Al. The experimental results show that {\alpha}-Al2O3 are thepossible nucleation sites for the Al3Sc cubes.

3D characterization of the primary Al3Sc phases in an Al-Sc alloy using Synchrotron X-ray tomography and electron microscopy