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A face-centered cubic (FCC) phase in electro-polished specimens fortransmission electron microscopy of commercially pure titanium has sometimesbeen reported. Here, a combination of atom-probe tomography, scanningtransmission electron microscopy and low-loss electron energy loss spectroscopyis employed to study both the crystal structural and chemical composition ofthis FCC phase. Our results prove that the FCC phase is actually a TiHx (x>1)hydride, and not a new allotrope of Ti, in agreement with previous reports. Theformation of the hydride is discussed.

Could face-centered cubic titanium in cold-rolled commercially-pure titanium only be a Ti-hydride?