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Intercalation of atomic species through epitaxial graphene layers began onlya few years following its initial report in 2004. The impact of intercalationon the electronic properties of the graphene is well known; however, theintercalant itself can also exhibit intriguing properties not found in nature.This suggests that a shift in the focus of epitaxial graphene intercalationstudies may lead to fruitful exploration of many new forms of traditionally 3Dmaterials. In the following forward-looking review, we summarize the primarytechniques used to achieve and characterize EG intercalation, and introduce anew, facile approach to readily achieve metal intercalation at thegraphene/silicon carbide interface. We show that simple thermalevaporation-based methods can effectively replace complicated synthesistechniques to realize large-scale intercalation of non-refractory metals. Wealso show that these methods can be extended to the formation of compoundmaterials based on intercalation. Two-dimensional (2D) silver (2D-Ag) andlarge-scale 2D gallium nitride (2D-GaNx) are used to demonstrate theseapproaches.

Epitaxial Graphene Intercalation: A Route to Graphene Modulation and Unique 2D Materials