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Polycrystalline samples of Fe2BiMO7 (M = Sb, Ta) compounds withpyrochlore-type structure were synthesized for the first time by the moltensalts method. The compounds were obtained in one hour at 950 C. The structureswere determined by Rietveld refinement. Through M\"ossbauer spectroscopy andX-ray photoelectron spectroscopy, the site occupancies and ionic states of thecations in the pyrochlore structure were investigated.Polycrystalline samplesof Fe2BiMO7 (M = Sb, Ta) compounds with pyrochlore-type structure weresynthesized for the first time by the molten salts method. The compounds wereobtained in one hour at 950 C. The structures were determined by Rietveldrefinement. Through M\"ossbauer spectroscopy and X-ray photoelectronspectroscopy, the site occupancies and ionic states of the cations in thepyrochlore structure were investigated.

M\"ossbauer and X-ray Photoelectron Spectroscopy Studies of Fe2BiMO7 (M = Sb, Ta) pyrochlore compounds synthesized by molten salts method