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An approach to visualize the accessible reciprocal space accounting thegoniometer angles limitation and the resolution element in the reciprocal spaceis presented. The shapes of the accessible reciprocal space region for coplanarand non-coplanar geometries are given employing the additional degree offreedom provided by detector arm. The examples of the resolution elements indifferent points of the reciprocal space are shown. The equations obtainedpermit to find these regions and to calculate the experimental geometry toobtain the diffraction from any accessible reflections, which makes a furtherextension of previously reported methods. The introduced algorithm has beentestified by experimental measurements of reciprocal space maps in coplanar andnon-coplanar geometries. The examples of the resolution elements in differentpoints of the reciprocal space are calculated to illustrate the methodproposed.

Computation and visualization of accessible reciprocal space and resolution element in high-resolution X-ray diffraction mapping