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In-plane ordering of Cs+ layers in Helmhotlz planes was studied on Pt(111)surface in 0.1 M CsF electrolyte solutions with synchtrotron surface x-rayscattering techniques. The ordering was measured in a new transmission cell,designed for in situ and non situ measurements and high-temperature sampleannealing all in the cell without sample transfer steps. At -850 mV vs.Ag/AgCl, (2x2) in-plane scattering peaks were weak under in situ condition andgrew rapidly under non situ condition as the surface emersed from theelectrolyte. The models for the (2x2) structures are presented and differencesbetween in situ and non situ conditions are discussed.

In situ and non situ surface x-ray scattering studies of in plane Cs+ ordering in Helmholtz planes of Pt(111) surface