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Nanostructures of Titanium oxide (TiO2) are being studied for many promisingapplications, e.g., solar photovoltaics, solar water splitting for H2 fuelgeneration etc., due to their excellent photo-catalytic properties. We havesynthesized low-dimensional TiO2 nanoparticles by gas phase CW CO2 laserpyrolysis. The laser synthesis process has been optimized for the deposition ofhighly pure, nearly mono-dispersed TiO2 nanoparticles on silicon substrates.Hard x-ray standing wave-field (XSW) measurements in total reflection geometrywere carried out on the BL-16 beamline of Indus-2 synchrotron radiationfacility in combination with x-ray reflectivity and grazing incidence x-rayfluorescence measurements for the determination of surface morphology of thedeposited TiO2 nanostructures. The average particle size of TiO2 nanostructureestimated using transmission electron microscopy (TEM) was found to closelyagree with the XSW and grazing incidence x-ray diffraction (GIXRD) results.

Determination of Surface Morphology of TiO2 nanostructure using synchrotron X-ray standing wave technique