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Amorphous nanoparticles (NPs) of diacetylene (DA) molecules were prepared byusing a reprecipitation method. After crystallization through solvent-vaporannealing process, the highly crystalline DA NPs show different structural andoptical characteristics compared with the amorphous DA NPs. The single crystalstructure of DA NPs was confirmed by high-resolution transmission electronmicroscopy (HR-TEM) and wide angle X-ray scattering (WAXS). The luminescencecolor and photoluminescence (PL) characteristics of the DA NPs were measuredusing color charge-coupled device (CCD) images and high-resolution laserconfocal microscope (LCM). The crystalline DA NPs emit bright green lightemission compared with amorphous DA NPs and the main PL peak of the crystallineDA NPs exhibits relative narrow and blue shift phenomena due to enhancedinteraction between DA molecular in the nano-size crystal structure.

Sharp and Bright Photoluminescence Emission of Single Crystalline Diacetylene Nanoparticles