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NiCo2O4 of varying nanostrucutures ranging from nanowires, nanoplates tonano-plates@nanowires were successfully grown on microporous (MP) Ni foams viaone-step hydrothermal process. The investigation of electrochemical capacitancefavors Ni-Co2O4 of nanoplates@nanowires microstructures which possessesspecific capacitance of 1380.3 F/g and 1033F/g at 5A/g and 50A/g respectivelyand 86.7% capacitance re-tention after 5000 cycles at 30A/g. The relationshipbetween morphology and specific capacitance was further explored by the modelof surface roughness factor (RF), which is indicative of the activeelectrode-electrolyte interface areas. The RF of porous Ni@NiCo2O4 wasremarkably improved by employing hierarchically porous (HP) Ni monoliths assubstrates, which illustrates the model of high energy density (12.6 F/cm2)electrodes for super-capacitors.

Hierarchically porous Ni monolith@branch-structured NiCo2O4 for high energy density supercapacitors