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A two step solid state reaction route has been presented to synthesizemonophasic cobalt tellurate (Co3TeO6, CTO) using Co3O4 and TeO2 as startingreagents. During synthesis, initial ingredient Co3O4 is found better than CoOin circumventing the intermediate Co5TeO8 or CoTeO3 phases. High resolutionSynchrotron X-ray Diffraction has been used to probe different phases presentin synthesized CTO and to achieve its single phase. Further, XANES studies nearCo K and Te L-edge reveal mixed oxidation states of Co (i.e. Co2+ and Co3+) and+VI valence state of Te respectively, which is also confirmed with XPS. Chargeimbalance due to different oxidation states of the Co-ions has been observed tobe compensated by plausible Te-cations vacancy. Enhanced multiferroicproperties like effective magnetic moment (JAP 116, (2014)) have beencorrelated with the present synthesis route.

Two step solid state synthesis and Synchrotron X-ray characterizations of ceramic Co3TeO6; an improper multiferroic