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The structural characterization of sol-gel based nano crystalline ZnOmaterial is being reported as we observe several previously unreportedstructural aspects following a sequence of annealing stages. As-grown sampleswere characterised by Fourier Transform Infrared Spectroscopy (FTIR). Chemicalpurity of the nano-grains and their crystallinity has been monitored by energydispersive X-ray (EDAX) analysis and transmission electron microscopy (TEM),while the unusual changes in nano-crystal growth structure have been studied byX-ray diffraction method. In addition, such samples have been studied by usingperturbed angular correlation (PAC) technique with the short-lived radioactiveprobe 111mCd. Changes in the local electronic environment following sinteringof the nano-crystalline grains have been observed by this method.

Gauging Structural Aspects of ZnO nano-Crystal Growth ThroughX-ray Diffraction Studies and PAC