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Systematic magnetic measurements have been performed in unique$\alpha -MnO_2$ square nanotubes synthesized by a facile hydrothermal method withmicrowave-assisted procedures. Unusual magnetic phenomena (abnormalmagnetization verse temperature (M - T) behaviour, large and abnormalmagnetization hysteresis loop horizontal shift (HHS) verse cooling field (HFC)behaviours (HHS - HFC) has been observed in these square nanotubes. Thesesuggest the observation of large unfrozen orbital moment which also is themicro -original of observed large and abnormal horizontal shift (HHS). Thefindings demonstrated that engineering layered structures in nanoscale wouldcreate many unique nanostructures and unusual physicochemical behaviours.

Abnormal Magnetic Behaviors in Unique Square alpha-MnO2 Nanotubes