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Nanoporous anatase TiO2 rods and rutile TiO2 chrysanthemums were successfullysynthesized via a simple ethylene glycol-mediated synthesis route. Theirmorphologies, phase compositions and components were characterized by SEM, TEM,Raman and IR, respectively. The results show that a self-assembly growth takesplace in the calcination under vacuum, which makes the titanium glycolate rodstransform into rutile TiO2/C chrysanthemums rather than anatase TiO2 rods. Italso indicates that the carbon plays an important role in the phase transitionprocess which promotes the phase transition to rutile TiO2 at a lowertemperature (400 oC). It provides a new approach to prepare nanoporous rutileTiO2 nanomaterials under low temperature.

Ethylene glycol-mediated synthesis of nanoporous anatase TiO2 rods and rutile TiO2 self-assembly chrysanthemums