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A novel potentiometric membrane sensor has been developed and optimized based on 3,5,13,15tetramethyl-4,14-diethyl-2,6,12,16,21,22-hexaazatricyclo [15.3. I 1-17 I 7-11 ] dicosa1,(21),2,5,7,19,11(22),12,15,17,19-decaene Cobalt Sulphate ionophore in poly vinyl chloride matrix membrane (PVC) plasticized with dibutyl phthalate (DBP), for high selective determination of iodide ion. The sensor works well in a linear range: 1.0×10 -2 – 1.0×10 -6 M with a Nernstian slope of -58.6 ±0.4 mV/decade and its detection limit is 8.0×10 -7 M. The sensor shows working range over the pH 3.0-9.5 and stable for a period of 2 months with response time <15 s. The selectivity coefficient values as determined by fixed interference method indicate a good selectivity for ions over a wide variety of other tested anions.

Highly Selective Iodide–Membrane Electrode Based On [CoL] SO4