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Interactions between Na2S 7H2O and Zn 2+ , Cd 2+ and Hg 2+ ions in solid state as well as in solution in presence of sun light ascertains tetrahedral structure instead of MxSy, with the help of their IR spectra, ESCA, TGA, DTA and XRD patterns. XRD patterns of cadmium and mercury compounds show possibility of two phases (α and β) of (Cd(H2O)3S) and (HgS)3H2O. Nanoparticles of ZnS, CdS and HgS were prepared in ethylene glycol indicating the particle size 10 - 20nm in TEM photograph. Keywords: ZnS, CdS and HgS Nanoparticles, ethylene glycol, TEM photograph

Interaction of Sodium Sulfide with Zn2+, Cd2+ and Hg2+ ions in Presence of Sun – light and Preparation of Nanoparticles in Ethylene glycol