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The spectroscopic methods of the different regions of the Electromagnetic spectrum are the most powerful and useful techniques available for the understanding of molecular structure, nature of bonding between atoms, confirmation analysis, symmetry of molecules, ions in crystals and so forth. The high resolution IR spectroscopic studies have recently received a great thrust due to the advent of advanced Fourier transform spectrometers. In the present investigation the spectral changes are studied in the vibrational spectra of thiourea, thiosemi carbazide in non aqueous solvent. The H2N stretching vibrations observed at 3371cm ̄1, 3259cm ̄1, & 3156cm ̄1 indicated that 3 different types of NH2 groups arising out of tautomeric form. The results obtained from the present study confirm that the solute – solvent interactions occurring in the solution is through intermolecular Hbonding.

Spectroscopic study on Thiourea and Thiosemicarbazide in Nonaqueous media