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This paper presents the effect of a synthesis method for cobalt catalyst supported on hydrotalcite material for Fischer-Tropsch synthesis. The hydrotalcite supported cobalt (HT-Co) catalysts were synthesized by co-precipitation and hydrothermal method. The prepared catalysts were characterized by using various techniques like BET (Brunauer–Emmett–Teller), SEM (Scanning Electron Microscopy), TGA (Thermal Gravimetric Analysis), XRD (X-ray diffraction spectroscopy), and FTIR (Fourier Transform Infrared Spectroscopy). Fixed bed micro reactor was used to test the catalytic activity of prepared catalysts. The catalytic testing results demonstrated the performance of hydrotalcite based cobalt catalyst in Fischer-Tropsch synthesis with high selectivity for liquid products. The effect of synthesis method on the activity and selectivity of catalyst was also discussed. Copyright © 2017 BCREC Group. All rights reserved Received: 3 rd November 2016; Revised: 26 th February 2017; Accepted: 9 th March 2017 ; Available online: 27 th October 2017; Published regularly : December 2017 How to Cite : Sharif, M.S., Arslan, M., Iqbal, N., Ahmad, N., Noor, T. (2017). Development of Hydrotalcite Based Cobalt Catalyst by Hydrothermal and Co-precipitation Method for Fischer-Tropsch Synthesis. Bulletin of Chemical Reaction Engineering & Catalysis , 12(3): 357-363 (doi:10.9767/bcrec.12.3.762.357-363)