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− H 5 PMo 10 V 2 O 40 (PMo 10 V 2 ) catalyst chemically immobilized on sulfur-containing mesoporous carbon (SMC) was prepared, and it was applied to the benzyl alcohol oxidation reaction. S-MC was synthesized by a templating method using SBA-15 and p-toluenesulfonic acid as a templating agent and a carbon precursor, respectively. S-MC was then modified to have a positive charge, and thus, to provide sites for the immobilization of PMo 10 V 2 . By taking advantage of the overall negative charge of [PMo 10 V 2 O 40 ], PMo 10 V 2 catalyst was immobilized on the S-MC support as a charge matching component. It was revealed that PMo 10 V 2 species were finely and molecularly dispersed on the S-MC via chemical immobilization. In the vapor-phase oxidation of benzyl alcohol, PMo 10 V 2 /S-MC catalyst showed higher conversion of benzyl alcohol and higher yield for benzaldehyde and benzoic acid than unsupported PMo 10 V 2 catalyst. The enhanced catalytic performance of PMo 10 V 2 /S-MC was due to fine dispersion of PMo 10 V 2 species on the S-MC via chemical immobilization.

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Benzyl Alcohol Oxidation over H5PMo10V2O40Catalyst Chemically Immobilized on Sulfur-containing Mesoporous Carbon