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TiO2 nanoparticles were successfully synthesized by the sol-gel method employing different glycols (ethylene glycol, diethylene glycol or polyethylene glycol 300), which were heat-treated in conventional oven or by hydrothermal via, obtaining photocatalysts with particle sizes and distinct crystalline structures. HRTEM analyses showed that the oxides submitted to hydrothermal treatment featured spherical morphology, being formed by partially aggregated particles with sizes varying between 2 and 5 nm. Xray diffractograms and Raman spectroscopy confirm that anatase was predominant in all synthesized compounds, with presence of brookite phase for samples that received hydrothermal treatment or were synthesized in the presence of polyethylene glycol with heat treatment in conventional oven. The amount of brookite as well as the cell volume, deformation, network parameters and crystallinity were estimated by Rietveld refinement. The surface area and porosity of the materials were higher when the synthesis involved the use of hydrothermal treatment. These oxides are mesoporous with porosity between 14 and 31%. The oxide synthesized in the presence of ethylene glycol with hydrothermal thermal treatment (TiO2G1HT) exhibited the highest photocatalytic activity in terms of mineralization of azo-dye Ponceau 4R (C.I. 16255), under UV-Vis irradiation. This higher photocatalytic activity can be attributed to the formation of binary oxides composed by anatase and brookite and by its optimized morphological and electronic properties. Subjects Catalysts, Ceramics, Nano and Microstructured Materials, Semiconductors

peerj

Synthesis of nano-TiO<sub>2</sub> assisted by glycols and submitted to hydrothermal or conventional heat treatment with promising photocatalytic activity

Synthesis of nano-TiO2 assisted by glycols and submitted to hydrothermal or conventional heat treatment with promising photocatalytic activity

Synthesis of nano-TiO₂ assisted by glycols and submitted to hydrothermal or conventional heat treatment with promising photocatalytic activity