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The present investigation describes the preparation, structural characterization studies on three different systems namely; system-I ((PMMA + PVDF)y – (Mg(CF3SO3)2)1-y), where 1-y = 60, 50, 40, 30 and 20 mol% respectively, System II ((PMMA + PVDF)y (Mg(CF3SO3)2)1-y)z-(EC)1-z, where 1-z = 25, 20, 15, 10 and 5 mol% respectively and System-III (((PMMA + PVDF)y (Mg(CF3SO3)2)1-y)z (EC)1-z)b (MgO)1-b ,where 1-b = 20, 15, 10 and 5 mol% respectively and these systems were prepared by solution-casting technique. In system-III the MgO nanofiller of 32 nm size prepared by wet chemical sol-gel method is added to arrive at nanocomposite solid polymer electrolyte systems in four different compositions namely 1-b = 20, 15, 10 and 5 mol% respectively. The synthesized MgO nanofiller size was confirmed by TEM study. Experimental techniques such as x-ray diffraction analysis, Fourier transform infrared spectroscopy (FTIR), differential scanning calorimetry (DSC) and surface morphological studies involving optical microscopy have been employed to explore their structural properties.

chemical science transactions

Synthesis and Structural Characterization Studies on Solid Polymer Electrolyte System with Magnesium Triflate as Host Salt, EC as Plasticizer and MgO as Nanofiller