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Mixed ligand Co(II), Ni(II) and Cu(II) complexes Co(EINA)2(PPD), Ni(EINA)2(PPD) and Cu(EINA)2(PPD), formed with ethyl-α-isonitrosoacetoacetate and dienes have been synthesized and characterized by their elemental analysis, infra red spectra and magnetic measurements. Ethyl-α- isonitrosoacetoacetate shows a tridentate behavior with coordination occurring through two oximino nitrogen atoms and further two coordination sides of metal ion are satisfied by oxygen atom. Diene acts as a bidentate ligand coordinating through the two nitrogen of the amino group.

Synthesis and Characterization of Mixed Ligand Complexes with Ethyl -α- Isonitrosoacetoacetate and Dienes