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Intramolecular cyclization of 3-propargylmercapto-1,2,4-triazole derivatives (2) to their corresponding 6-methyl thiazolo(3,2-b)(1,2,4)triazoles (3) was affected in the presence of nano catalyst, Fe(HSO 4)3/TiO 2 as solid acid in high yields.

chemical science transactions

Fe(HSO4)3 Supported on Nano-TiO2 : An Efficient Heterogeneous Catalyst for Intramolecular Cyclization of 3-Propaygylmercapto Triazoles to 6-Methyl-thiazolo[3,2-B][1,2,4]triazoles