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Intercalation behaviors of alkali metals into natural graphite flakes in the solutions of dimethoxymethane (DMM) and diethoxymethene (DEM) containing alkali metals have been investigated bymeans of X-ray diffraction.Ternary graphite intercalation compounds (GICs) containing lithium were obtained from the solutions of Li-DMMand Li-DEM. On the other hand, binary GICs were prepared from those solutions for K, Rb and Cs. Sodium did notdissolve into the solvents.

Preparation of Alkali Metal-graphite Intercalation Compounds in the Solutions of Alkali Metals Dissolved in Dimethoxymethane or Diethoxyethane