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New carboranyl substituted sulfonamide porphyrins were synthesized in good yields by the reaction of amino group of 5-(p-aminophenyl)-10,15,20-triphenylporphyrin with carboranylsulfonyl chlorides prepared in situ by oxidative chlorination of corresponding mercapto carborane with trichloroisocyanuric acid in MeCN–H2O system. The reactions were carried out under mild conditions. The structure of all compounds obtained was confirmed by means of electronic, IR, 1Н and 11B NMR spectroscopy and mass spectrometry. Quantum-chemical studies by DFT calculations were carried out for synthesized porphyrin derivatives.

Synthesis of Sulfonamide Derivatives of Carboranyl Porphyrins Based on 5-(4-Aminophenyl)-10,15,20-triphenylporphyrin and Mercapto Carboranes