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Homotrinuclear complexes were synthesized by reaction of [30]trithiadodecaazahexaphyrine (hemihexaphyrazine) with nickel(II), copper(II) or manganese(II) acetates in phenol. The compounds were characterized by UV-Vis, IR spectroscopy, mass-spectrometry and elemental analysis. Study of thermal behavior of manganese complex has shown high thermal stability. The structure of a cationic copper complex observed in mass-spectrum was elucidated by quantum chemistry calculations at the DFT level.

Homotrinuclear Сomplexes of [30]Trithiadodecaazahexaphyrine with Transition Metals: Ni(II), Cu(II) and Mn(II)