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Methods are presented for the preparation of d-glucos e-6-t , d-xylose- 5-t , and d-mannitol- 1 - t by the reduction of suitable compounds with lithium borohydride- t in anhydrous tetrahydrofuran, followed by hydrolysis of the products. The starting materials for the reductions are, respectively, 1,2- O -isopropylidene-d-glucurono-6,3-lactone, 5-aldo-1,2- O -isopropylidene-d- xylo -pentofuranose, and 2,3:5,6-di- O -isopropylidene-d-mannofuranose. The apparatus and procedure for carrying out the reductions in a closed system are described.

Tritium-labeled compounds IV. D-glucose-6-t, d-xylose-5-t, and d-mannitol-1-t