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An apparatus is described for growing single crystals in a small droplet of melt at temperatures up to 1,600° C. The droplet, held by capillarity at the junction of a thermocouple, can be observed during the process through a binocular microscope. The heating is by means of a high-frequency current that can be separated by a filter from the thermocouple electromotive force, allowing the electromotive force to be measured continuously. The apparatus is therefore suitable also for determining melting points. <i The process of mounting and grinding the single-crystal specimens for X-ray diffraction and a simple but versatile micromanipulator to facilitate these procedures are described.

Techniques for growing and mounting small single crystals of refractory compounds