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This paper deals with errors in volumetric gas analysis caused by the displacement of nitrogen from and its solution in liquid reagents when these are used to remove a reactive gas from a gas mixture. The data show that measurable volumes of nitrogen may be exchanged between the gas sample and the reagent, as well as between the atmosphere and the reagent at the surface of separation in the atmospheric arm of the absorption pipette. Volumetric errors may also result from the change of solubility of nitrogen in the reagent with temperature when heat is liberated during the absorption of a reactive gas. Errors from these sources are roughly proportional to the solubility of nitrogen in the reagents. CONTENTS Page

Displacement of nitrogen from and its solution in certain reagents during volumetric gas analysis