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Transference numbers, measured by the moving boundary method, must be corrected for the change in volume which occurs at the electrode on the closed side of the transference cell. It has been customary to compute this volume correction from the densities of the electrode materials and of the solution, together with a value for the transference number. A method for measuring the volume correction is described. Measurements of the correction to be applied in the case of a silver-silver chloride electrode ic potassium chloride solution show that the computed value is correct up to concentrations of 0.2 molal, to within the precision required.

bureau of standards journal of research

Note on the moving boundary method for measuring transference numbers - A pycnometer for determining the volume change occurring at an electrode and its application to a cathode of silver chloride in a solution of potassium chloride