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Inclusion-separation and preconcentration of dioxin from blood samples were reported by the inclusion-facilitated emulsion liquid membrane process. The novelty of this study is the application of nano-baskets of calixarene as well as emulsion liquid membranes in the selective and efficient preconcentration of dioxin. For this aim, inclusion-extraction parameters of four p-tert-calix[4]arene derivatives sulfonamide moieties previously synthesized were investigated. Analysis by a gas chromatograph revealed that under the optimized operating condition, the preconcentration of dioxin was improved and the method achieved lower limit of detections.

Separation and Preconcentration of Dioxin in Blood Samples by Nano-baskets of Calixarene and Inclusion Emulsion Membranes