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Win this paper we report the stoichiometric reduction of carbon monoxide coordinated to a metal, by hydrogen (hydride) using a homogeneus ionic system formed by combining two ionic complexes suche as [MoH3 (PMePh2) 3]+ or [WH5 (PMePh2)4]+ with [Rh12 (CO)34]2- or [Co (CO)4]- in polar medium acting  as solvent. In a atmosphere os synthesis-gas, using pressures from 5 to 100 atms. and temperatures from 25 to 200°C a detectable amount of ethylene glycol were produced and identified by gas-liquidi-chromatography (g.l.c.), infrared, 1H n.m.r. and gas chromatography - mass spectra (G.C./M.S.).

Obtenção de etileno glicol a partir de CO e H2 usando soluções homogêneas de hidretos catiônicos de Mo e W com carbonilas aniônicas de Rh e Co