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The short-range structural parameters for NaNO2 and KNO2 pure melts were determined by the time-of-flight neutron diffraction. The precise analyses of structural parameters obtained such as coordination number, interatomic distance, and temperature factor allowed us to conclude that (1) there exist stable NO2− anions in the melts, (2) NO2− anions behave like NO3− anions due to the existence of lone pairs of electrons, (3) the short-range structure of KNO2 pure melt is similar to that of NaNO2 pure melt but the cation site relative to anion is a little different from each other in terms of the cation size effect.

Pulsed Neutron Diffraction Study of NaNO2 and KNO2 Pure Melts