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The methanol dissociative adsorption at a Pt-loading carbon (Pt/C) electrocatalyst for direct methanol fuel cell has been investigated by electrochemical measurements using a porous microelectrode (PME) and porous/disk-dual microelectrode (P/D-ME). The proton elimination reaction based on the methanol dissociative adsorption during the primary process of the methanol electrooxidation on a Pt/C surface, especially at Pt(100), has been observed by PME measurements. Furthermore, by using the P/D-ME, we have succeeded for the first time in the electrochemical detection of protons dissociated from methanol molecules into the bulk solution due to the above reaction.

Electrochemical Detection of Methanol Dissociative Adsorption at Pt/C Surface by Using Porous-Microelectrodes