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Advanced 2D carbon materials such as graphene and derivatives are basic building blocks for future nanostructured generation in electronics and energy horizons owing to their remarkable physical and chemical properties. In this context, production scalability of 2D materials having high purity with distinctive and multi-functionalities, that facilitate in fundamental research and advanced studies as well as in industrial applications. A variety of techniques have been employed to develop 2D advanced carbon materials, amongst state-of-the-art synthetic protocols, electrochemical is deliberated as a promising approach that provides high yield, great performance, low cost, and excellent up-scalability. Notably, playing with electrochemical parameters not only allows tunable properties but also enhances the content variety from graphene to a wide spectrum of 2D semiconductors. In this chapter, a succinct and comprehensive survey of recent progress in electrochemical exfoliation routes and presents the processing techniques, strategic design for exfoliations, mechanisms, and electrochemistry of graphene.

Electrochemical Exfoliation of 2D Advanced Carbon Derivatives