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In the early to mid-90’s, NMR studies were being published that recognized the power of magic angle spinning (MAS) to increase resolution in materials that were not strictly solids by averaging differences in magnetic susceptibility and residual dipolar coupling inherent in these samples. The method of utilizing MAS for non-solid materials to produce liquid-like NMR lines was termed High-Resolution Magic Angle Spinning (HR-MAS). A few of the first HR-MAS examples included investigation of resins for combinatorial chemistry,[1] solvent swollen polystyrene gels,[2] and lipid systems.[3] Then in 1996, Maas et al. [4] advanced the field of HR-MAS NMR by adding a magnetic field gradient along the magic angle (see Figure 1). Like high resolution solution NMR, this gradient improved sensitivity and resolution with the ability to more easily select coherence pathways and by reducing indirect dimension (t1) noise.[4]

HR-MAS NMR Spectroscopy in Material Science