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The synthesis of inorganic non-stoichiometric compounds such as thermostable fibrous fluorosilicates of amphibole group shaped in form of fibrous-acicular crystals represents one of the perspective directions in the modern materials science. The importance of fibrous amphiboles, including synthetic fibrous fluorosilicates (FFS) derives from multifunctionality and specificity of their properties. They are elastic, flexible, and resistant to aggressive media, have high mechanic strength, low electric and heat conductance, heat and fire resistance, express an ability to absorb certain gases and liquids, etc. By present, fibrous amphiboles and their synthetic counterparts in pure state or composed with other substances (pitch, rubber, cement, ceramics, carbon fluoride) are widely used in various fields of modern industry and technique. The main consumers of fibrous silicates and fibrous-based composites are chemical and electro-technical industries, the manufacturing of fillers for electrolytic chambers and for acid dampers, the production of electrical wires, plastic and rubber for special purposes, paints, clays, varnishes, lubricants in the motor-car, aircraft, ship-building, and rocket plants. In atomic power engineering these compounds are used as structuring and insulting materials (Khachatryan, 1969; Hawkins, 1971; Grigor’eva et al., 1975; Li, 1992, Tareev, 2002-2011).

The Solid-Phase Synthesis of the Inorganic Non-Stoichiometric Compounds-Fibrous Fluorosilicates