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The main focus of this Chapter was targeted on novel approaches to compatibility of particles with polymer matrices and detail analysis of rheology-morphology interrelationships. Rather attractive method of mixing based on knowledge of rheological behavior of polymers at high shear rates was proposed and studied. The major fraction of ND around 40 nm and absence of agglomerates of micron dimensions allow us to recommend this method for industrial application. For successful processing of nanocomposite precursors interrelationships between rheological properties and stream morphology is extremely important and depending on the task, it is possible to obtain either chaotic or regular distribution of filler particles. These data were obtained by combining rheological and optical or structural methods. Hypothesis over the main driving force of particles ordering based on regular elastic instability of polymer matrix causing ordering of particles was proposed. Mechanical characterization confirms the strong influence of dimensional homogeneity of particles on final properties of nanocomposites

Rheology-Morphology Interrelationships for Nanocomposites based on Polymer Matrices