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R2 Fig. 1. Chemical structure of s-triazine core, substituent in R1 : Cl, SCH3 or OCH3; R2 and R3: hydrocarbons chains. These herbicides have been extensively applied to pre and post-emergence weed control. Many studies were focused on ecological and health hazards of these compounds and their toxic effects are very well known. For this reason, the use of some triazine pesticides has been banned in some countries or their permitted levels in drinking water is very low, so that analytical procedures for quantitative determination of several triazines, as well as their degradation products, at low levels are often requested. In this sense, several analytical techniques have been developed, like HPLC (Katsumata et al., 2006), CG-MS, capillary electrophoresis (Frias et al., 2004), solid-phase micro-extraction coupling with GC, LC, ion mobility spectrometry (Garcia Galan et al., 2010; Mohammadi et al., 2009; Sanchez Ortega et al., 2009; Quintana et al., 2001) and with HPLC (Zhou et al.,

An Electrochemical Approach to Quantitative Analysis of Herbicides and to the Study of Their Interactions with Soils Components