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Pre-blends and pre-mixes.—Mixtures of one or more food additives, with food materials or all other carriers, and not intended for direct consumption by humans. Limit of quantitation (LOQ).—The minimum concentration or mass of analyte in a given matrix that can be reported as a quantitative result. Repeatability.—Variation arising when all efforts are made to keep conditions constant by using the same instrument and operator, and repeating during a short time period. Expressed as the repeatability standard deviation (SDr); or % repeatability relative standard deviation (%RSDr). Reproducibility.—The standard deviation or relative standard deviation calculated from among-laboratory data. Expressed as the reproducibility standard deviation (SDR); or % reproducibility relative standard deviation (%RSDR). Recovery.—The fraction or percentage of spiked analyte that is recovered when the test sample is analyzed using the entire method. 4 Method Performance Requirements

AOAC SMPR 2012.003: Standard Method Performance Requirements for Vitamin A in Pre-Blends, Pre-Mixes, and Pure Materials