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We wish to report a novel preparation method for Gemsurf analogs as well as dicarboxylic acid-type Gemini surfactant from Diels-Alder adducts of 2-trimethylsilyloxy-1,3-butadiene, in which ozone oxidation is adopted to convert C=C double bond to dicarboxylic acid without any additional oxidant.

Preparation of Dicarboxylic Acid - Type Gemini Surfactant via Diels-Alder Reaction ^|^amp; Ozone Oxidation