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Products of titanium dissolution in the active state are investigated in fluoride contain­ing 1 M H 2 SO 4 solutions. The novel method of dual dynamic voltammetry, applied to Ti disk/Pt ring rotating ring–disk electrodes, is utilized for the simultaneous detection of different dissolution products. Potential regions where certain products (primarily, Ti III and H 2 ) are formed are identified by a 3D electrochemical map constructed based on the ring–disk electrode measurements. Besides dissolution in the form of Ti III species and hydrogen evolution, the formation and prompt oxidation of Ti II can also be presumed under the applied conditions.

Investigating products of titanium dissolution in the presence of fluoride ions with dual dynamic voltammetry