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Microstructural properties of six samples, prepared by rapid hydrolysis of aluminum secbutoxide,were investigated at RT using field emission scanning electron microscopy (FE SEM), X-raypowder diffraction (XRD) and Fourier transform infrared (FT-IR) spectrometry. The results of structuralanalysis show that, regardless of a significant difference in the processing parameters (pH, temperature,time of synthesis), all products contain boehmite as the only crystal phase present. The results of FE-SEManalysis indicate a significant difference in the morphology of obtained boehmites (plates, needles, granules).The results of line-broadening analysis of powder diffraction patterns (Le Bail method – programGSAS) indicate the presence of very small anisotropic crystal domains (around 1.5 to 7 nm in the direction010; around 3 to 16 nm in the direction perpendicular to 010). In all cases the parameters that contributeto the strain broadening of diffraction lines decrease to nearly zero, which suggests that the obtainedboehmites are almost strain-free. (doi: 10.5562/cca1884

Microstructural Analysis of Boehmite Nanoparticles Prepared by Rapid Hydrolysis of Aluminum Sec-butoxide