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The mixed adsorption layers of tetramethylthiourea and a cationic detergent formed at electrodesurface in NaClO4 (1 mol dm–3) are described. The systems were characterized by the measurement of differentialcapacity, zero charge potential, and surface tension at this potential. The data were analyzed toobtain the surface pressure and relative surface excess of tetramethylthoiurea as a function of electrodecharge at bulk concentration of studied compounds. It was stated that the adsorbing tetramethylthoiureamolecule pushed out the water molecule instead of the detergent molecule from the electrode surface.The constants of the Frumkin and corrected Flory-Huggins isotherm point to a decreased TMTU adsorptionenergy in the cationic detergents presence and stronger repulsive interaction. Electrostatic parametersof the inner layer were assigned. In the range of more negative potentials, mixed adsorptionlayers were described by investigating the kinetics of the Zn2+ ions electroreduction as a piloting ion.(doi: 10.5562/cca1791

Adsorption of Tetramethylthiourea in the Presence of Cationic Detergent at Interface Electrode / Aqueous Perchlorate Solutions