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The intermetallic zinc compounds CaAuZn, SrPdZn, SrPtZn, SrAuZn, BaPd 1.57  Zn 3.43 , and BaAu 1.41 Zn 3.59  were synthesized from the elements in sealed niobium ampoules in an induction furnace. The equiatomic compounds crystallize with the orthorhombic TiNiSi-type structure, space group Pnma. Single-crystal X-ray data exhibited small degrees of Au=Zn mixing within the three-dimensional [AuZn] networks and resulted in the compositions CaAu 1.02 Zn 0.98  and SrAu 1.03 Zn 0.97  for two investigated single crystals. BaPd 1.57  Zn 3.43  and BaAu 1.41  Zn 3.59  adopt partially ordered versions of the LT-SrZn 5  type, space group Pnma. Both structures were refined on the basis of X-ray single-crystal diffractometer data. a=1331.13(6), b=531.45(3), c=682.20(4) pm, wR=0.0245, 1138 F 2  values, 39 variables for BaPd 1.57 Zn 3.43  and a=1344.35(2), b=537.47(2), c=691.22(4) pm, wR=0.0441, 931 F 2  values, 37 refined variables for BaAu 1.41 Zn 3.59 . The transition metal and zinc atoms form a complex three-dimensional network of (T, Zn) 4  tetrahedra which are condensed via common corners and T/Zn-T/Zn bonds. Large cavities within these networks are filled by the barium atoms which have coordination number 19, i. e. Ba@(T, Zn) 17 Ba 2 .

New Intermetallic Zinc Compounds with Ordering Variants of the KHg 2 and LT-SrZn 5 Type