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Block- and platelet-shaped single crystals of several CeNi 1-x Sb 1+y Bi 1-y  phases with ZrCuSiAstype structure (space group P4=nmm) were grown from a CeNiSb precursor in bismuth fluxes. The structures of CeNiSb 1.19 Bi 0.81 , CeNi 0.80 Sb 1.16 Bi 0.84  and CeNi 0.75 Sb 1.74 Bi 0.26  were refined from single-crystal X-ray diffractometer data. The 2b nickel site can be fully or partially occupied, and the bismuth square nets show solid solutions with antimony. CaBe 2 Ge 2- type CeNi 2-x Sb 2  crystals occur as by-products of the crystal growth experiments. The structure of a CeNi 1.26 Sb 2  crystal has been refined. The small difference of the compositions hamper phase analytical studies by powder X-ray diffraction. A polycrystalline CeNiSbBi sample showed Curie-Weiss behavior with an experimental magnetic moment of 2.56(1) μ B  per Ce atom, indicating purely trivalent cerium. No magnetic ordering is detected down to 2:5 K. A  121 Sb Mössbauer spectrum showed an isomer shift of δ = -8.06(6)mms -1 , substantiating the antimonide character.

CeNi 1-x Sb 1+y Bi 1-y Phases with ZrCuSiAs-type and CeNi 1.26 Sb 2 with CaBe 2 Ge 2 -type Structure