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Transparent and colorless single crystals of Yb 26 B 12 O 57  were obtained by reacting Yb 2 O 3  and B powder at 1000 °C in the presence of a KCl flux for 24 h in silica-jacketed Nb ampoules and subsequent removal of the flux by washing with water. Yb 26 B 12 O 57  crystallizes in the monoclinic space group C2/m (no. 12, Z = 1) with the lattice parameters a = 2454:1(3), b = 357:78(4), c = 1426:7(2) pm and β = 115:111(6)°, and its structure differs slightly from that of a known compound with the same stoichiometry. Raman spectra of single crystals of the title compound were recorded and compared to those of known borate compounds

An Alternative Crystal Structure of Yb 26 B 12 O 57 – X-Ray Structure Determination on Flux-synthesized Single Crystals