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We report the synthesis and crystal structure of the monohydrate of hexaammine copper(II) difluoride, [Cu(NH 3 ) 6 ]F 2  · H 2 O, which was synthesized from CuF 2  · 2 H 2 O in liquid ammonia. The compound crystallizes in the chiral space group P3 2 21 (no. 154) as traffic-blue, plate-shaped crystals with a = 6.738(1), c = 18.210(6) Å, V = 715.9(3) Å3 at 150 K with Z = 3. It contains the rare [F(H 2 O)F 2-  anion bound by strong O-H···F hydrogen bonding.

The Hexaammine Copper(II) Fluoride Monohydrate [Cu(NH 3 ) 6 ][F(H 2 O)F]: Synthesis and Crystal Structure