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Two d 10  metal coordination polymers with bis-benzimidazole ligands, [(Ag(L 1 ))·NO 3 ·4H 2 O] n  (1) and [Cu 2 (L 2 )(CN) 2 ] n  (2) [L 1  =1,4-bis(benzimidazol-1-yl)butane, L 2  =1,4-bis(5,6-dimethylbenzimidazol- 1-yl)butane] have been synthesized hydrothermally and characterized by elemental analysis, IR spectroscopy, thermogravimetric (TG) analysis and single-crystal X-ray diffraction. Compound 1 features a ribbon-like chain structure bridged by L1 ligands, and is ultimately extended into a 2D supramolecular network through two kinds of π-π stacking interactions. Compound 2 displays a (6,3) wave-like layer in which [Cu 6 (μ-CN) 6 (L 2 ) 2 ] n  double chains are interconnected by pairs of L 2  bridges. The fluorescence properties of the compounds in the solid state at room temperature were investigated.

Synthesis, Crystal Structures and Fluorescence Properties of Two d10 Metal Coordination Polymers with Flexible Bis(benzimidazolyl)alkane Ligands